The only in Russia small and macromolecule single crystal structure analysis system equipped with a rotating anode X-ray source (flux 8 × 1010 phot/mm²/с) and a curved imaging plate detector allowing collecting high-quality data from weakly diffracting and disordered crystals.

 

Technical charachteristics

  • • Microfocused X-ray generator MicroMax™-007 HF with rotating (Co or Mo) source.
  • • Power of X-ray sources – 1.2 kW.
  • • Detector – cylindrical IP with vertical translation axis and 2θ range of 204o:
  •           • radius – 127.4 mm;
  •           • readout time – 51 sec;
  •           • erase time – 20 sec;
  •           • sensitivity – 2 ADU/X-ray photon.
  • • 3-axis goniometer:
  •           • ω axis – -85° to 265° 0.002° /step;
  •           • χ axis – -15° to 55° 0.0002° /step;
  •           • φ axis – 360° 0.002° /step;
  • • Conofocal X-ray optics VariMax™.
  • • Camera: 1/3" camera for sample alignment and observation; 70X magnification color image displayed on host computer.
  • • Low-temperature Oxford Cryostream system with temperature range 80-500 K.

Software

  • CrystalClear™ automated measurement/processing software.
  • Software for face indexing using CCD video camera.
  • TwinSolve twinned crystal integration software.
  • CrystalStructure™ single-crystal structure solution refinement and reporting suite.

Information from the manufacturer:

http://www.rigaku.com/products/smc/rapid
http://www.rigaku.com/downloads/journal/Vol15.2.1998/rapid.pdf
http://www.rigaku.com/downloads/journal/Vol16.2.1999/uekusa.pdf

Location:

The Vasilyevsky Island training and research Complex of SPbSU.